HRID322552

反应详情

EQUATION

反应方程式

HRID 322552 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
0 °C

PROCEDURE

实验过程

To a solution of Boc—Arg(Tos)—Thiazole (300 mg, 0.6 mmol) in CH2Cl2 (10 mL) at 0° C. was added TFA (10 mL). The solution was stirred at 0° C. for 2 h. The solvent and excess TFA were evaporated to an oily residue which was used directly without further purification in Example 6.

WORKUP

后处理

  1. customThe solvent and excess TFA were evaporated to an oily residue which
  2. customwas used directly without further purification in Example 6