HRID322552
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
CONDITIONS
反应条件
- 温度
- 0 °C
PROCEDURE
实验过程
To a solution of Boc—Arg(Tos)—Thiazole (300 mg, 0.6 mmol) in CH2Cl2 (10 mL) at 0° C. was added TFA (10 mL). The solution was stirred at 0° C. for 2 h. The solvent and excess TFA were evaporated to an oily residue which was used directly without further purification in Example 6.
WORKUP
后处理
- customThe solvent and excess TFA were evaporated to an oily residue which
- customwas used directly without further purification in Example 6