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HRID32307

反应详情

EQUATION

反应方程式

HRID 32307 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)(C)OC(=O)N1CCCC(C(=O)Nc2ccccc2)C1
HCID18104216

未命名化合物

PRODUCTS

生成物

1
结构：Cl.O=C(Nc1ccccc1)C1CCCNC1
HCID16303570

N-Phenylpiperidine-3-carboxamide--hydrogen chloride (1/1)

C12H17ClN2O

收率 55%

PROCEDURE

实验过程

A solution of 1-t-butoxycarbonyl-3-piperidinecarboxanilide (437 mg, 1.43 mmol) and hydrochloride (1 ml, 4.00 mmol, 4N ethyl acetate) was stirred for several hours. Filtration of the precipitate gave 3-piperidinecarboxanilide hydrochloride (187 mg, 55%).

WORKUP

后处理

  1. filtrationFiltration of the precipitate