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HRID326912

反应详情

EQUATION

反应方程式

HRID 326912 的结构方程式

REACTANTS

反应物

3
结构：CCO
HCID702

Ethanol

C2H6O

结构：O=Cc1cccc(C=Cc2ccc3ccc(Cl)cc3n2)c1
HCID53394853

3-[2-(7-Chloro-2-quinolinyl)ethenyl]benzaldehyde

C18H12ClNO

结构：C[Mg+].[Br-]
HCID178418689

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)c1cccc(C=Cc2ccc3ccc(Cl)cc3n2)c1
HCID54221497

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

To 3-(2-(7-chloro-2-quinolinyl)ethenyl)benzaldehyde, MeMgBr was added (in THF at 0° C.) to give an ethanol derivative, which was oxidized to the title compound as in Example 15, Step 11. 1H NMR (CD3COCD3): δ 2.68 (3H, s), 7.55-7.68 (3H, m), 7.89-8.05 (6H, m), 8.36 (2H, m).