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HRID32746

反应详情

EQUATION

反应方程式

HRID 32746 的结构方程式

REACTANTS

反应物

3
结构：OC1CCCNC1
HCID23293

3-Piperidinol

C5H11NO

结构：CNS(=O)(=O)c1ccc(Cl)c(C(=O)O)c1
HCID111724

Benzoic acid, 2-chloro-5-[(methylamino)sulfonyl]-

C8H8ClNO4S

结构：CS(=O)(=O)c1ccc(N2CCCC2)c(C(=O)O)c1
HCID59793489

未命名化合物

PRODUCTS

生成物

1
结构：CNS(=O)(=O)c1ccc(N2CCCC(O)C2)c(C(=O)O)c1
HCID59793580

未命名化合物

收率 15%

PROCEDURE

实验过程

The title compound was synthesised according to the procedure described for the synthesis of 5-Methanesulfonyl-2-pyrrolidin-1-yl-benzoic acid (Example S) from 2-Chloro-5-methylsulfamoyl-benzoic acid and rac-3-hydroxy-piperidine and obtained in 15% yield. MS (m/e): 312.9 (MH− 100%).

WORKUP

后处理

  1. customobtained in 15% yield