HRID328559

反应详情

EQUATION

反应方程式

HRID 328559 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
75 °C

PROCEDURE

实验过程

Magnesium glycinate was prepared by reacting 4 grams of glycine with 2.5 grams of basic magnesium carbonate (26.3% Mg) in 30 grams of water while agitating at 75° C. for one half hour. The cooled mixture was then added to 77 grams of zirconyl chloride (13.6% Zr) with stirring. To the above solution 100 grams of 50% aluminum chlorhydroxide (12.5% Al) was added with agitation. The mixture was heated at 85° C. for 20 minutes. The product was then evaporated at 53° C. under a vacuum of 200 mm of Hg and contained 15.8% Al, 13.6% Mg. 5.3% glycine and 22.1% Cl.

WORKUP

后处理

  1. stirringwith stirring
  2. temperatureThe mixture was heated at 85° C. for 20 minutes
  3. customThe product was then evaporated at 53° C. under a vacuum of 200 mm of Hg