HRID333430

反应详情

EQUATION

反应方程式

HRID 333430 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

91 mg (0.29 mmol) of tert-butyl 3-(2-methylcyclohexyl)-3-propoxyazetidine-1-carboxylate are dissolved in 8 mL of dichloromethane. The reaction medium is immersed in an ice bath. 2 mL of trifluoroacetic acid are added. After 1 hour, the solvents are evaporated off. 113 mg in the form of a brown oil are used in the following step without further purification.

WORKUP

后处理

  1. customThe reaction medium is immersed in an ice bath
  2. customthe solvents are evaporated off
  3. custom113 mg in the form of a brown oil are used in the following step without further purification