HRID334089

反应详情

EQUATION

反应方程式

HRID 334089 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
200 °C

PROCEDURE

实验过程

A mixture of 123 mg (0.284 mmol) [4-(4-amino-3-methylamino-benzoyl)-2,2-dimethyl-piperazin-1-yl]-(1-phenyl-1H-[1,2,4]-triazol-3-yl)-methanone and 500 μL (3.99 mmol) cyclopentylacetic acid was stirred at 200° C. for 30 min. The reaction mixture was diluted with DMF and purified by HPLC.

WORKUP

后处理

  1. custompurified by HPLC