HRID336380

反应详情

EQUATION

反应方程式

HRID 336380 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

100 mg 3,5-bis-(4-fluoro-phenyl)-1H-(1,2,4)triazole, 111 mg 2-bromo-1-(4-pyrimidin-2-yl-piperazin-1-yl)-ethanon and 237 mg potassiumcarbonat in 5 mL acetone was stirred 24 h at RT. The reaction was filtered and the filtrate was evaporated. The residue was crystallized with acetonitrile to yield 124 mg of the desired compound.

WORKUP

后处理

  1. filtrationThe reaction was filtered
  2. customthe filtrate was evaporated
  3. customThe residue was crystallized with acetonitrile