HRID339599

反应详情

EQUATION

反应方程式

HRID 339599 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Prepared as described in the Nitro Reduction section using 2-(4-{(E)-2-[4-nitro-2-(2-fluoroethoxy)phenyl]ethenyl}phenyl)-6-methylimidazo[1,2-a]pyridine (81 mg, 0.194 mmol) and tin (II) dichloride dihydrate (219 mg, 0.970 mmol) in EtOH (12 ml) to give the title compound (36 mg, 48%) as an orange solid after work-up and flash chromatography (2:1 EtOAc/DCM).

WORKUP

后处理

  1. customPrepared