反应详情

To a stirring solution of 1-azido-3-phenyl-propan-2-ol (590 mg, 3.4 mmol) in 20 mL methanol under a nitrogen atmosphere was added 10 mg of Pd(OH)2/C (10%). Hydrogen gas was delivered via balloon. The solution was stirred overnight at room temperature. The catalyst was removed by filtering the solution through a bed of celite, and the filtrate was concentrated to give a clear oil under reduced pressure. M+1=152.

1. customThe catalyst was removed
2. filtrationby filtering the solution through a bed of celite
3. concentrationthe filtrate was concentrated
4. customto give a clear oil under reduced pressure