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HRID33983

反应详情

EQUATION

反应方程式

HRID 33983 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C(OC(Cl)(Cl)Cl)OC(Cl)(Cl)Cl
HCID94429

Triphosgene

C3Cl6O3

结构：COc1cc(N)c(C(=O)N2CCCC2C(C)(C)O[SiH2]C(C)(C)C)cc1OC
HCID131727079

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(N=C=O)c(C(=O)N2CCCC2C(C)(C)O[SiH2]C(C)(C)C)cc1OC
HCID131727078

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

2 次

PROCEDURE

实验过程

A solution of triethylamine (1.35 eq.) in anhydrous toluene was added to the amine (5)(1 eq.) and triphosgene (0.36 eq.) in anhydrous toluene under a N2 atmosphere. The reaction was finished after 2 hours. (monitored by IR, ξNCO 2265 cm1). The product was used without further purification.

WORKUP

后处理

  1. customThe product was used without further purification