Sodium Bicarbonate → HCID 53729413, compound

HRID 341748Notes

Reaction equation

HRID 341748 reaction equation
Cl[CH:2]1[S:6][CH2:5][N:4]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)[C:3]1=[O:13].C(=O)(O)[O-:15].[Na+]>O1CCCC1>[OH:15][CH:2]1[S:6][CH2:5][N:4]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)[C:3]1=[O:13]

Participants

4

Reactant 2

HCID 516892Sodium BicarbonateHCID 54121276HCID 54121276, compound

Product 1

HCID 53729413HCID 53729413, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

By a procedure similar to that described in Preparative Example 2, Step 3 above, but using 5-chloro-3-phenyl-4-thiazolidinone (prepared as in Step 2 above), tetrahydrofuran (10 ml) and saturated aqueous sodium bicarbonate (15 ml), the title compound was obtained as an oily solid, yield 0.24 g.

Sources & evidence

ORD record
ord-f13ccb3a2f4d4b979568c10cefa171ad
Source dataset
uspto-grants-1999_01
Patent number
US05856273

Reaction notes

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