Potassium Carbonate → HCID 67703355, compound

HRID 343293Notes

Reaction equation

HRID 343293 reaction equation
[Cl:1][C:2]1[N:6]([CH:7]([CH3:9])[CH3:8])[C:5]([CH3:10])=[N:4][C:3]=1[C:11]1[CH:16]=[CH:15][C:14]([OH:17])=[CH:13][CH:12]=1.Cl[CH2:19][C:20]1[CH:32]=[CH:31][C:30]([CH2:33][CH3:34])=[CH:29][C:21]=1[O:22][CH:23]([CH3:28])[C:24]([O:26][CH3:27])=[O:25].C(=O)([O-])[O-].[K+].[K+]>CN(C)C=O>[CH2:33]([C:30]1[CH:31]=[CH:32][C:20]([CH2:19][O:17][C:14]2[CH:13]=[CH:12][C:11]([C:3]3[N:4]=[C:5]([CH3:10])[N:6]([CH:7]([CH3:9])[CH3:8])[C:2]=3[Cl:1])=[CH:16][CH:15]=2)=[C:21]([CH:29]=1)[O:22][CH:23]([CH3:28])[C:24]([O:26][CH3:27])=[O:25])[CH3:34]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 53722094HCID 53722094, compoundHCID 53874087HCID 53874087, compound

Product 1

HCID 67703355HCID 67703355, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

This compound is prepared in a manner analogous to that of Step I of Example 1, using 0.75 gram (0.0030 mole) of 4-[5-chloro-1-(1-methylethyl)-2-methylimidazol-4-yl]phenol, 0.84 gram (0.0036 mole) of methyl 2-(2-chlormethyl-5-ethylphenoxy)propanoate (prepared in Steps A through C of Example 1), and 0.62 gram (0.0045 mole) of potassium carbonate in N,N-dimethylformamide, yielding the title compound.

Workup

  1. customThis compound is prepared in a manner analogous to that of Step I of Example 1

Sources & evidence

ORD record
ord-744d7293c3d84c1da080680ed8bb5795
Source dataset
uspto-grants-1999_01
Patent number
US05861359

Reaction notes

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