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HRID344407

反应详情

EQUATION

反应方程式

HRID 344407 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1ccc(Cl)c(Cl)c1
HCID22710

3,4-Dichlorobenzaldehyde

C7H4Cl2O

结构：COc1cc(N)c(Cl)cc1C(=O)NCC1CCN(CCCCCCN)CC1
HCID53683637

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(N)c(Cl)cc1C(=O)NCC1CCN(CCCCCCNCc2ccc(Cl)c(Cl)c2)CC1
HCID53706175

未命名化合物

收率 50.7%

PROCEDURE

实验过程

4-Amino-N-(1-(6-aminohexyl)piperidin-4-ylmethyl)-5-chloro-2-methoxybenzamide (2.0 g) as starting compound and 3,4-dichlorobenzaldehyde (0.97 g) were reacted and treated in the same manner as in Example 121 to give 1.42 g of 4-amino-5-chloro-N-((1-(6-(3,4-dichlorobenzylamino)hexyl)piperidin-4-yl)methyl)-2-methoxybenzamide.

WORKUP

后处理

  1. customwere reacted
  2. additiontreated in the same manner as in Example 121