p-Toluenesulfonic acid → HCID 57197078, compound

HRID 344589Notes

Reaction equation

HRID 344589 reaction equation
[CH2:1]([C:4]1[C:9]([OH:10])=[CH:8][CH:7]=[CH:6][C:5]=1[N:11]1[C:15](=[O:16])[C:14]2[CH2:17][CH2:18][CH2:19][CH2:20][C:13]=2[C:12]1=[O:21])[CH:2]=[CH2:3].CC1C=CC(S(O)(=O)=O)=CC=1>C1(C)C(C)=CC=CC=1>[CH3:3][CH:2]1[CH2:1][C:4]2[C:5]([N:11]3[C:15](=[O:16])[C:14]4[CH2:17][CH2:18][CH2:19][CH2:20][C:13]=4[C:12]3=[O:21])=[CH:6][CH:7]=[CH:8][C:9]=2[O:10]1

Participants

4

Reactant 2

HCID 6101p-Toluenesulfonic acidHCID 15018889HCID 15018889, compound

Product 1

HCID 57197078HCID 57197078, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

Example 2 was prepared, as a yellow oil, by treating 0.48 g of 1D with PTSA in xylene according to the procedures described in Example 1.

Workup

  1. customExample 2 was prepared, as a yellow oil

Sources & evidence

ORD record
ord-5eba8b71d4104d83956c5ff8149b2c9c
Source dataset
uspto-grants-1991_10
Patent number
US05053071

Reaction notes

Loading…