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HRID345005

反应详情

EQUATION

反应方程式

HRID 345005 的结构方程式

REACTANTS

反应物

5
结构：O=C(n1ccnc1)n1ccnc1
HCID68263

1,1'-Carbonylbis(1H-imidazole)

C7H6N4O

结构：NCCN1CCOCC1
HCID408285

2-Morpholinoethylamine

C6H14N2O

结构：CCc1cn(C(c2ccccc2)(c2ccccc2)c2ccccc2)cn1
HCID19358858

未命名化合物

结构：COC(=O)c1cccc(F)c1[N+](=O)[O-]
HCID19432020

Methyl 3-fluoro-2-nitrobenzoate

C8H6FNO4

结构：[Al+3].[H-].[H-].[H-].[H-].[Li+]
HCID21226445

未命名化合物

PRODUCTS

生成物

1
结构：CCc1cnc2c(=O)[nH]c3c(CNCCN4CCOCC4)cccc3n12
HCID19809400

未命名化合物

PROCEDURE

实验过程

Treat 3-fluoro-2-nitrobenzoic acid methylester with 1-trityl-4-ethyl imidazole, followed by treatment with 4-(2-aminoethyl)morpholine and catalytic hydrogenation cyclization with carbonyldiimidazole, followed by reduction with lithium aluminum hydride to provide the title compound.