反应详情

温度

210 °C

Anthracene (89.0 gm) was combined with methyl acrylate (51.5 gm) and xylenes (500 ml) in a Parr bomb and heated to 210° C. for 12 hours. The solvent was removed on a rotary evaporator and the residue was recrystallized from methanol to provide the product as a white solid (m=113-114° C.).

1. customThe solvent was removed on a rotary evaporator
2. customthe residue was recrystallized from methanol