Methyl Acrylate → 13294-86-5

HRID 345019Notes

Reaction equation

HRID 345019 reaction equation
[CH:1]1[C:14]2[C:5](=[CH:6][C:7]3[C:12]([CH:13]=2)=[CH:11][CH:10]=[CH:9][CH:8]=3)[CH:4]=[CH:3][CH:2]=1.[C:15]([O:19][CH3:20])(=[O:18])[CH:16]=[CH2:17]>>[CH:4]1[C:5]2[CH:6]3[CH2:17][CH:16]([C:15]([O:19][CH3:20])=[O:18])[CH:13]([C:12]4[C:7]3=[CH:8][CH:9]=[CH:10][CH:11]=4)[C:14]=2[CH:1]=[CH:2][CH:3]=1

Participants

3

Reactant 2

HCID 7294Methyl AcrylateHCID 8418Anthracene

Product 1

HCID 27580413294-86-5

Conditions

Temperature
210 °C

Procedure

Anthracene (89.0 gm) was combined with methyl acrylate (51.5 gm) and xylenes (500 ml) in a Parr bomb and heated to 210° C. for 12 hours. The solvent was removed on a rotary evaporator and the residue was recrystallized from methanol to provide the product as a white solid (m=113-114° C.).

Workup

  1. customThe solvent was removed on a rotary evaporator
  2. customthe residue was recrystallized from methanol

Sources & evidence

ORD record
ord-64fd0738b05d494c8dcf5bded802c83c
Source dataset
uspto-grants-1991_10
Patent number
US05055468

Reaction notes

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