Cyanuric chloride → HCID 88511634, compound

HRID 346002Notes

Reaction equation

HRID 346002 reaction equation
[N:1]1[C:8]([Cl:9])=[N:7][C:5](Cl)=[N:4][C:2]=1[Cl:3].[CH3:10][C:11]1([CH3:27])[CH2:16][CH:15]([NH:17][CH2:18][CH2:19][CH2:20][CH2:21][C:22](=[O:24])[CH3:23])[CH2:14][C:13]([CH3:26])([CH3:25])[NH:12]1>C1(C)C(C)=CC=CC=1>[Cl:9][C:8]1[N:1]=[C:2]([Cl:3])[N:4]=[C:5]([N:12]2[C:13]([CH3:25])([CH3:26])[CH2:14][CH:15]([NH:17][CH2:18][CH2:19][CH2:20][CH2:21][C:22](=[O:24])[CH3:23])[CH2:16][C:11]2([CH3:27])[CH3:10])[N:7]=1

Participants

4

Reactant 2

HCID 7954Cyanuric chlorideHCID 21615603HCID 21615603, compound

Product 1

HCID 88511634HCID 88511634, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

9.2 g of cyanuric chloride and 26.7 g of 2,2,6,6-tetramethyl-4-(N-acetylbutylamino)-piperidine are reacted in 100 ml of xylene as described in Example 1 and worked up. 2,4-Dichloro-6-[2,2,6,6-tetramethyl-4-(N-acetylbutylamino)-piperidin-1-yl)-1,3,5-triazine is obtained as colorless crystals having a melting point of 131°-133°.

Sources & evidence

ORD record
ord-1fba8ae993bf4cffafb940019987ed69
Source dataset
uspto-grants-1991_10
Patent number
US05059689

Reaction notes

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