反应详情

13.6 g (0.1 mole) of 1-phenylpropan-1-ol are taken up in petroleum ether and are reacted at -20° C. with hydrochloric acid until the precipitation of water is terminated. Subsequently, the organic phase is washed neutral with water, dried (sodium sulfate) and the petroleum ether removed in a vacuum. The bright yellow, thermolabile oil is used without further purification. The oil has an Rf of 0.8 (CH2Cl2) and is attained in a yield of 13.1 g (85%).

1. customis terminated
2. washSubsequently, the organic phase is washed neutral with water
3. dry with materialdried (sodium sulfate)
4. customthe petroleum ether removed in a vacuum
5. customThe bright yellow, thermolabile oil is used without further purification