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HRID35084

反应详情

EQUATION

反应方程式

HRID 35084 的结构方程式

REACTANTS

反应物

2
结构：CCCN1C(=O)C2(c3ccc([N+](=O)[O-])cc3)CC(c3ccc([N+](=O)[O-])cc3)(C2)C1=O
HCID14872621

未命名化合物

结构：CCOCC.ClCCl
HCID21881112

未命名化合物

PRODUCTS

生成物

1
结构：CCCN1C(=O)C2(c3ccc(N)cc3)CC(c3ccc(N)cc3)(C2)C1=O
HCID20027820

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

In a manner analogous to that described in Example 12a, 0.4 g of 1,5-di-(4-nitrophenyl)-3-n-propyl-3-azabicyclo[3.1.1]heptane-2,4-dione are dissolved in 15 ml of ethyl acetate, hydrogenated in the presence of 80 mg of 5% palladium-on-carbon and worked up. Melting point 149°-150° (from ether/methylene chloride).