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HRID35396

反应详情

EQUATION

反应方程式

HRID 35396 的结构方程式

REACTANTS

反应物

2
结构：COC(OC)N(C)C
HCID78373

Methanamine, 1,1-dimethoxy-N,N-dimethyl-

C5H13NO2

结构：COc1ccc(C(C)(C)C)cc1S(N)(=O)=O
HCID10933694

ST50778292

C11H17NO3S

PRODUCTS

生成物

1
结构：COc1ccc(C(C)(C)C)cc1S(=O)(=O)N=CN(C)C
HCID54498328

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

4.68 g (0.02 mole) of 3-(1,1-dimethylethyl)-6-methoxybenzenesulfonamide are dissolved in 50 ml of dimethylformamide, and 2.5 g (0.022 mole) of dimethylformamide dimethylacetal are added. The mixture is left to stand for 30 minutes at room temperature and is poured into ice water and the product is filtered off with suction.

WORKUP

后处理

  1. waitThe mixture is left
  2. filtrationthe product is filtered off with suction