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HRID355033

反应详情

EQUATION

反应方程式

HRID 355033 的结构方程式

REACTANTS

反应物

3
结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：O=c1[nH]c2cc([N+](=O)[O-])ccc2o1
HCID263965

5-Nitro-1,3-benzoxazol-2(3H)-one

C7H4N2O4

结构：COC(=O)CCCCCCCBr
HCID11107373

Methyl 8-bromooctanoate

C9H17BrO2

PRODUCTS

生成物

1
结构：COC(=O)CCCCCCCn1c(=O)oc2ccc([N+](=O)[O-])cc21
HCID12961164

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

The product is produced as described in example 1 from 6 g. of NaH (80% suspension in mineral oil), 36 g. of 5-nitrobenzoxazolin-2-one (produced in usual manner by reacting 2-amino-4-nitrophenol-hydrochloride with phosgene), 400 cc. of DMF, 47.4 g. of 8-bromo caprylic acid methyl ester and 6 g. of NaJ.

WORKUP

后处理

  1. customThe product is produced