1,2-Epoxybutane → HCID 19601722, compound

HRID 355558Notes

Reaction equation

HRID 355558 reaction equation
[C:1]([C:3]1[CH:4]=[C:5]([OH:9])[CH:6]=[CH:7][CH:8]=1)#[N:2].[CH3:10][CH2:11][CH:12]1[O:14][CH2:13]1.O.[OH-].[Li+]>>[C:1]([C:3]1[CH:4]=[C:5]([CH:6]=[CH:7][CH:8]=1)[O:9][CH2:13][CH:12]([OH:14])[CH2:11][CH3:10])#[N:2]

Participants

4

Reactant 3

HCID 78341,2-EpoxybutaneHCID 133943-CyanophenolHCID 168937Lithium hydroxide, monohydrate

Product 1

HCID 19601722HCID 19601722, compound

Procedure

is obtained analogously to Example H1 by using 20.7 g of 3-cyanophenol, 13.8 g of α-butylene oxide and 0.5 g of lithium hydroxide monohydrate in a yield of 25.9 g in the form of an oil; b.p. 116°-118° C./0.04 torr.

Sources & evidence

ORD record
ord-595e71bd45484c92a8580ebae1a2f7fc
Source dataset
uspto-grants-1998_11
Patent number
US05831114

Reaction notes

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