HRID357057

反应详情

EQUATION

反应方程式

HRID 357057 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 1.15 g (3.65 mmol) of 5-butylidene-3-[2-(imidazo[1,2-a]pyridin-5-yl)ethyl]thiazolidine-2,4-dione in 50 ml of methanol, 0.33 ml of concentrated hydrochloric acid was added. After the solvent was distilled off, the residue was washed with diethyl ether to yield 1.00 g (77.9%, light yellow solid) of the desired product.

WORKUP

后处理

  1. distillationAfter the solvent was distilled off
  2. washthe residue was washed with diethyl ether