HRID357180

反应详情

EQUATION

反应方程式

HRID 357180 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 77 mg (0.23 mmol) of 5-ethylidene-3-[4-(imidazo[1,2-a]pyridin-5-ylthio)butyl]oxazolidine-2,4-dione in 5 ml of methanol, 0.10 ml of concentrated hydro-chloric acid was added. After the solvent was distilled off, the residue was washed with diethyl ether to yield 90 mg (quant., brown oily substance) of the desired product.

WORKUP

后处理

  1. distillationAfter the solvent was distilled off
  2. washthe residue was washed with diethyl ether