HRID35991
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A mixture of ethanolamine, trityl chloride and pyridine was refluxed for 15 h. Water was added slowly to the cooled reaction and the precipitate collected by filtration. The crude product recrystallized from a 1:1 mixture of ethanol and water.
WORKUP
后处理
- temperaturewas refluxed for 15 h
- filtrationthe precipitate collected by filtration
- customThe crude product recrystallized from a 1:1 mixture of ethanol and water