HRID362399

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6893

2,3-Xylidine

C8H11N

结构：O=C(Cl)c1ccc(C(=O)N2Cc3ccccc3Cc3ccccc32)cc1

HCID53802244

未命名化合物

PRODUCTS

生成物

结构：Cc1cccc(NC(=O)c2ccc(C(=O)N3Cc4ccccc4Cc4ccccc43)cc2)c1C

HCID15307992

未命名化合物

收率 98.8%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

As described for Example 123, a mixture of 0.361 g of 4-[(6,11-dihydro-5H-dibenz[b,e]azepin-5-yl)carbonyl]benzoyl chloride, 0.101 g of triethylamine and 0.145 g of 2,3-dimethylaniline is stirred for 1.5 hr. and worked up to give 0.44 g of crystals, m.p. 248°-251° C.