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HRID364196

反应详情

EQUATION

反应方程式

HRID 364196 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CCN(CC)CCNN
HCID3028735

Ethanamine, N,N-diethyl-2-hydrazino-

C6H17N3

结构：O=c1c2cc(OCc3ccccc3)ccc2sc2c([N+](=O)[O-])ccc(Cl)c12
HCID20240232

未命名化合物

PRODUCTS

生成物

1
结构：CCN(CC)CCn1nc2c3c(c([N+](=O)[O-])ccc31)Sc1ccc(OCc3ccccc3)cc1-2
HCID20240225

未命名化合物

收率 61.1%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1C
溶剂HCID7237

o-Xylene

C8H10

PROCEDURE

实验过程

A mixture of 1.2 g (0.0091 mol) of 2-(diethylaminoethyl)hydrazine, 2.7 g (0.0069 mol) of 1-chloro-4-nitro-7-phenylmethoxy-9H-thioxanthen-9-one, and 0.97 g (0.0069 mol) of powdered K2CO3 in 30 ml of xylene was reacted and 2.0 g of the product was isolated as described in Example 58.

WORKUP

后处理

  1. customwas reacted