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HRID364894

反应详情

EQUATION

反应方程式

HRID 364894 的结构方程式

REACTANTS

反应物

1
结构：CN(C)C=NS(=O)(=O)c1cc(C(C)(C)C)cc(CNC(=O)CCl)c1O
HCID53948117

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)c1cc(CN)c(O)c(S(N)(=O)=O)c1.Cl
HCID21296905

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：Cl
溶剂HCID313

Hydrochloric Acid

ClH

结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

3 g (0.008 mole) of 2-chloro-N-[5-(1,1-dimethylethyl)-3 -dimethylaminomethyleneaminosulfonyl-2-hydroxybenzyl]-acetamide in a mixture of 30 ml of ethanol and 3 ml of concentrated hydrochloric acid are heated under reflux for 2 hours. The solvent is removed in vacuo and the residue is crystallized from methanol/ether.

WORKUP

后处理

  1. temperatureare heated
  2. temperatureunder reflux for 2 hours
  3. customThe solvent is removed in vacuo
  4. customthe residue is crystallized from methanol/ether