Benzaldehyde → 5-Phenyl-2,4-Pentadienol

HRID 370582Notes

Reaction equation

HRID 370582 reaction equation
[CH:1](=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:9](=[O:18])[CH:10]=[CH:11][C:12]1C=CC=CC=1>C(Cl)(Cl)Cl>[C:2]1([CH:1]=[CH:12][CH:11]=[CH:10][CH2:9][OH:18])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 240BenzaldehydeHCID 3073-Phenylprop-2-Enal

Product 1

HCID 534270135-Phenyl-2,4-Pentadienol

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

Analysis by GC and MS showed the major component to have m/e 160. Minor impurities included benzaldehyde and cinnamaldehyde. IR (CHCl3): cm-1 3620 (s), 3430 (br, OH), 3020 (s), 1650 (m), 1620 (m), 1600 (m).

Sources & evidence

ORD record
ord-3941c0e58f3d4fd09bbd89565b27ccc0
Source dataset
uspto-grants-1985_07
Patent number
US04526993

Reaction notes

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