HRID370717

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID66057

2-Methylpiperazine

C5H12N2

结构：CC(C)n1cc(C(=O)O)c(=O)c2cc(F)c(F)c(F)c21

HCID13477692

未命名化合物

PRODUCTS

生成物

结构：CC1CN(c2c(F)cc3c(=O)c(C(=O)O)cn(C(C)C)c3c2F)CCN1

HCID13477664

未命名化合物

收率 48.2%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

A mixture of 0.68 g of 6,7,8-trifluoro-1,4-dihydro-1-isopropyl-4-oxoquinoline-3-carboxylic acid, 0.72 g of 2-methyl piperazine and 10 ml of pyridine was treated in the same manner as described for Example 4 to give 0.42 g of the title compound as colorless crystals. M.p. 217°-218° C.

WORKUP

后处理

additionwas treated in the same manner