Hydrochloric Acid → Dodecylamine hydrochloride

HRID 371254Notes

Reaction equation

HRID 371254 reaction equation
[CH2:1]([NH2:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[ClH:14]>C(Cl)Cl>[ClH:14].[CH2:1]([NH2:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 13583Dodecylamine

Product 1

HCID 458426Dodecylamine hydrochlorideYield 95.5%

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Conditions

Temperature
0 °C

Procedure

Dodecylamine (85 g, 0.46 mol) was dissolved in methylene chloride (500 mL). The solution was cooled to 0° C., and saturated with anhydrous hydrogen chloride (45 minutes). The white, crystalline solid was separated and dried in vacuum over phosphorus pentoxide, to provide 97.5 g (95.5%) of n-dodecylamine hydrochloride.

Workup

  1. customThe white, crystalline solid was separated
  2. dry with materialdried in vacuum over phosphorus pentoxide

Sources & evidence

ORD record
ord-3610f441decb46118ba667e34d25705d
Source dataset
uspto-grants-1985_07
Patent number
US04530714

Reaction notes

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