HRID371726

反应详情

EQUATION

反应方程式

HRID 371726 的结构方程式

PROCEDURE

实验过程

In an analogous manner as described in Example 2, 1-aminomethyl-1-cyclohexane-acetic acid hydrochloride is reacted with methanol in the presence of hydrogen chloride. After evaporation in a vacuum the residue is recrystallised from methanol/ether to give pure methyl 1-aminomethyl-1-cyclohexane-acetate; m.p. 150° - 152° C. (hydrochloride)

WORKUP

后处理

  1. customAfter evaporation in a vacuum the residue
  2. customis recrystallised from methanol/ether