HRID372003

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID24654

Hydrazine hydrate (1:1)

H6N2O

HCID10060312

Benzenebutanoic acid, 3-chloro-4-methoxy-gamma-oxo-

C11H11ClO4

PRODUCTS

产物

HCID10823876

未命名化合物

收率 84%

PROCEDURE

实验过程

This compound was prepared in 84% yield by reaction of 3-(3-chloro-4-methoxybenzoyl)propionic acid with hydrazine hydrate in ethanolic solution at reflux temperature for 5 hours. It had mp 194°-195° C after crystallisation from ethanol.

WORKUP

后处理

temperatureat reflux temperature for 5 hours
customafter crystallisation from ethanol