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HRID373320

反应详情

EQUATION

反应方程式

HRID 373320 的结构方程式

REACTANTS

反应物

2
结构：c1ccc(N2CCNCC2)cc1
HCID7096

Phenylpiperazine

C10H14N2

结构：CN(C)C(OCC(C)(C)C)OCC(C)(C)C
HCID78623

N,N-Dimethylformamide dineopentyl acetal

C13H29NO2

PRODUCTS

生成物

1
结构：CC(C)(C)COC(OCC(C)(C)C)N1CCN(c2ccccc2)CC1
HCID19812302

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

A solution of 4-phenylpiperazine (0.162 g, 0.001 mol) and dimethylformamide dineopentyl acetal (0.346 g, 0.0015 mol) in anhydrous chloroform (5 mL) was refluxed for 10 hours. The solvent and excess reagent were removed (100° C./1 mm) to give the product in quantitative yield.

WORKUP

后处理

  1. customThe solvent and excess reagent were removed (100° C./1 mm)
  2. customto give the product in quantitative yield