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HRID374576

反应详情

EQUATION

反应方程式

HRID 374576 的结构方程式

REACTANTS

反应物

3
结构：C[N+](=O)[O-]
HCID6375

Nitromethane

CH3NO2

结构：CC(=O)[O-].[NH4+]
HCID517165

Ammonium acetate

C2H7NO2

结构：O=Cc1cn(Cc2ccc(Cl)cc2)c2ccccc12
HCID872445

1-[(4-Chlorophenyl)methyl]-1H-indole-3-carbaldehyde

C16H12ClNO

PRODUCTS

生成物

1
结构：O=[N+]([O-])C=Cc1cn(Cc2ccc(Cl)cc2)c2ccccc12
HCID896590

1-[(4-Chlorophenyl)methyl]-3-(2-nitroethenyl)-1H-indole

C17H13ClN2O2

PROCEDURE

实验过程

80.9 g of 1-(4-chlorobenzyl)-3-formylindole, prepared in Example 5, 18 g of ammonium acetate and 300 ml of nitromethane are refluxed for 30 min.

WORKUP

后处理

  1. temperatureare refluxed for 30 min.