反应详情

In dimethylformamide, 0.05 mol of 9,10-diaminoanthracene, 0.35 mol of p-nitroiodobenzene, 0.14 mol of anhydrous potassium carbonate, and copper powder were added and refluxed with stirring for 4 days. After the reaction was completed, the reaction mixture was filtered, and the filtered product was thoroughly washed with dimethylformamide, water and acetone, followed by drying. Thus, 0.043 mol of brown tetrakis(p-nitrophenyl)-9,10-diaminoanthracene was obtained.

1. temperaturerefluxed
2. filtrationthe reaction mixture was filtered
3. washthe filtered product was thoroughly washed with dimethylformamide, water and acetone
4. customby drying