HRID377510

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8079

Cyclohexene

C6H10

HCID20312

4,6-Dichloro-5-nitropyrimidine

C4HCl2N3O2

HCID66130

1H-Imidazole, 2-ethyl-

C5H8N2

HCID68263

1,1'-Carbonylbis(1H-imidazole)

C7H6N4O

HCID566323

N,1-Dimethylpiperidin-4-amine

C7H16N2

PRODUCTS

生成物

结构：CCc1ncc2c(=O)[nH]c3c(NCC4CCN(C)CC4)ncnc3n12

HCID70270934

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID23938

Palladium

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Prepared by treatment of 4,6-dichloro-5-nitropyrimidine with 1-methyl-4-(methylamino)piperidine followed by reaction with 2-ethylimidazole, reduction with palladium on carbon and cyclohexene in refluxing ethanol, and cyclization with carbonyidiimidazole.