反应详情

温度

115 °C

A mixture of 10.0 g (67.1 mmol) of 4,6-dichloropyrimidine and 5.7 g (67.1 mmol) of piperidine in 100 ml of water is stirred at a bath temperature of 115° C. for 16 h. After cooling to RT, the precipitate is filtered off, washed with water and dried under reduced pressure.

1. temperatureAfter cooling to RT
2. filtrationthe precipitate is filtered off
3. washwashed with water
4. customdried under reduced pressure