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HRID379730

反应详情

EQUATION

反应方程式

HRID 379730 的结构方程式

REACTANTS

反应物

2
结构：Cc1cccc(C(=O)CBr)c1
HCID10036129

2-Bromo-1-(3-methylphenyl)ethan-1-one

C9H9BrO

结构：CCOC(=O)Nc1cc(Cl)ccc1C#N
HCID18367888

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)n1c(C(=O)c2cccc(C)c2)c(N)c2ccc(Cl)cc21
HCID18368043

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in step 2 of Example 1 from 4-chloro-2-(ethoxycarbonylamino)benzonitrile (Example 1, step 1) and 2-bromo-3′-methylacetophenone (R. Yveline, G. Gerard, and M. Geroges, Chem.Pharm.Bull., 1992, 40, 1170.). tlc: Rf=0.5 (25% ethyl acetate in hexanes)