Potassium Bromide → HCID 18368088, compound

HRID 379799Notes

Reaction equation

HRID 379799 reaction equation
[C:1]([NH:4][C:5]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[N:7](C(OCC)=O)[C:6]=1[C:19](=[O:26])[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)(=[O:3])[CH3:2].[K+].[Br-]>>[C:1]([NH:4][C:5]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[NH:7][C:6]=1[C:19](=[O:26])[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 253877Potassium BromideHCID 18367824HCID 18367824, compound

Product 1

HCID 18368088HCID 18368088, compound

Procedure

The title compound was prepared according to the procedure described in step 2 of Example 2 (Method A) from 3-acetylamino-2-benzoyl-1-(ethoxycarbonyl)indole (step 1). 1H-NMR (CDCl3) δ: 9.78 (1H, br s), 8.24 (1H, d, J=8 Hz), 8.22 (1H, br s), 7.82 (2H, d, J=8 Hz), 7.64-7.52 (3H, m), 7.42-7.25 (2H, m), 7.16 (1H, t, J=8 Hz), 2.26 (3H, s) IR (KBr) ν: 3360, 1670, 1620, 1540, 730 cm−1

Sources & evidence

ORD record
ord-fe8b63a8940048269dd4300a4d14e12a
Source dataset
uspto-grants-2001_10
Patent number
US06300363B1

Reaction notes

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