HRID38262

反应详情

EQUATION

反应方程式

HRID 38262 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1-(5-chloro-2-methoxyphenyl)-piperazine hydrochloride (8 g) was heated in a solution of 48% aqueous HBr (200 ml) and the mixture was heated at reflux for 99 hours. The reaction mixture was concentrated in vacuo, the sub-title compound was used directly without any further purification.

WORKUP

后处理

  1. temperaturethe mixture was heated
  2. temperatureat reflux for 99 hours
  3. concentrationThe reaction mixture was concentrated in vacuo
  4. customthe sub-title compound was used directly without any further purification