HRID38262
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
1-(5-chloro-2-methoxyphenyl)-piperazine hydrochloride (8 g) was heated in a solution of 48% aqueous HBr (200 ml) and the mixture was heated at reflux for 99 hours. The reaction mixture was concentrated in vacuo, the sub-title compound was used directly without any further purification.
WORKUP
后处理
- temperaturethe mixture was heated
- temperatureat reflux for 99 hours
- concentrationThe reaction mixture was concentrated in vacuo
- customthe sub-title compound was used directly without any further purification