HRID385737

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(C)(O)c1ccc(-c2cc(C(N)=O)c([N+](=O)[O-])s2)cn1

HCID59525801

5-[6-(1-Hydroxy-1-methylethyl)-3-pyridinyl]-2-nitro-3-thiophenecarboxamide

C13H13N3O4S

PRODUCTS

生成物

结构：CC(C)(O)c1ccc(-c2cc(C(N)=O)c(N)s2)cn1

HCID59526287

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID23939

Platinum

溶剂HCID887

Methanol

CH4O

2 次

PROCEDURE

实验过程

To 5-[6-(1-hydroxy-1-methylethyl)pyridin-3-yl]-2-nitrothiophene-3-carboxamide (245 mg, 0.80 mmol) in MeOH (20 mL) was added 3% Pt/C doped with 0.6% V (52 mg, 8.0 μmol). The reaction was stirred under a hydrogen balloon at room temperature for 4 h. The solution was diluted with MeOH, filtered through Celite, and evaporated to give the title compound as a gray solid.

WORKUP

后处理

filtrationfiltered through Celite
customevaporated