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HRID3878

反应详情

EQUATION

反应方程式

HRID 3878 的结构方程式

REACTANTS

反应物

1
结构：COc1cc(C(N)=O)ccc1-c1nc2[nH]c(=O)[nH]c(=O)c2[nH]1
HCID20153243

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(C#N)ccc1-c1nc2[nH]c(=O)[nH]c(=O)c2[nH]1
HCID20153256

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O=P(Cl)(Cl)Cl
溶剂HCID24813

Phosphoric trichloride

Cl3OP

PROCEDURE

实验过程

Prepared by boiling 0.7 gm of 8-(2-methoxy-4-aminocarbonylphenyl)-1H,3H-purin-2,6-dione in 10 ml of phosphorus oxychloride for 24 hours. The compound crystallizes as the hemihydrate.

WORKUP

后处理

  1. customPrepared
  2. customfor 24 hours
  3. customThe compound crystallizes as the hemihydrate