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HRID394489

反应详情

EQUATION

反应方程式

HRID 394489 的结构方程式

REACTANTS

反应物

2
结构：COC(C)(OC)N(C)C
HCID87835

1,1-Dimethoxyethyl(dimethyl)amine

C6H15NO2

结构：NC(=S)c1ccc(SCCCCOc2cccc(C(F)(F)F)c2)nn1
HCID18176642

未命名化合物

PRODUCTS

生成物

1
结构：CC(=NC(=S)c1ccc(SCCCCOc2cccc(C(F)(F)F)c2)nn1)N(C)C
HCID18176643

未命名化合物

收率 100%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

A mixture of intermediate 12 (0.009 mol) and N,N-dimethylacetamide dimethyl acetal (0.015 mol) in toluene (100 ml) was stirred and refluxed for 3 hours. The solvent was evaporated, yielding 4.1 g (100%) of N-[1-(dimethylamino)ethylidene]-6-[[4-[3-(trifluoromethyl)phenoxy]butyl]thio]-3-pyridazinecarbothioamide (intermediate 13).

WORKUP

后处理

  1. temperaturerefluxed for 3 hours
  2. customThe solvent was evaporated