Hydrochloric Acid → 1-(3'-Chlorophenyl)-3-methyl-1H-pyrazole

HRID 394777Notes

Reaction equation

[Cl:1][C:2]1[CH:3]=[C:4]([NH:8][NH2:9])[CH:5]=[CH:6][CH:7]=1.Cl.[C:11]1(NN)[CH:16]=CC=[CH:13][CH:12]=1>>[Cl:1][C:2]1[CH:3]=[C:4]([N:8]2[CH:16]=[CH:11][C:12]([CH3:13])=[N:9]2)[CH:5]=[CH:6][CH:7]=1

Participants

Reactant 3

HCID 313Hydrochloric Acid

HCID 7516Phenylhydrazine

HCID 75332(3-Chlorophenyl)hydrazine

Product 1

HCID 179200861-(3'-Chlorophenyl)-3-methyl-1H-pyrazole

Procedure

This compound was prepared by the same methodology described for EXAMPLE 1 with 3-chlorophenyl hydrazine.HCl substituted for phenyl hydrazine. There was obtained the title compound; HRMS (M+H)+: calc. 467.094465; found 467.091517.

Workup

customThis compound was prepared by the same methodology

Sources & evidence

ORD record: ord-5b9e889d055045749ae83fe5f84e15ca
Source dataset: uspto-grants-2003_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06602895B2

Reaction notes

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