HRID400484

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID9321

Hydrazine

H4N2

HCID73896

1,3-Propanedione, 1,3-bis(4-fluorophenyl)-

C15H10F2O2

PRODUCTS

生成物

HCID16105479

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8028

Tetrahydrofuran

C4H8O

CONDITIONS

反应条件

温度: 75 °C

PROCEDURE

实验过程

3.9 g 1,3-Bis-(4-fluoro-phenyl)-1,3-propandione was dissolved in 45 mL of a solution of 1 N hydrazine in THF and stirred for 2 h at 75° C. The solvent was removed to give 3.6 g of the desired compound. Rt: 1.03 min (method D), (M+H)+: 257

WORKUP

后处理

customThe solvent was removed