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HRID406776

反应详情

EQUATION

反应方程式

HRID 406776 的结构方程式

REACTANTS

反应物

3
结构：O=C(OC(Cl)(Cl)Cl)OC(Cl)(Cl)Cl
HCID94429

Triphosgene

C3Cl6O3

结构：Cc1cc([C@H](C)N)ccc1Br
HCID58102381

未命名化合物

结构：C[C@@H](c1ccc(-c2ccn(C)c(=O)c2)cc1)N1CCC(CC(C)(C)O)(C2CC2)OC1=O
HCID59635673

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc([C@H](C)N=C=O)ccc1Br
HCID86649416

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The title compound was prepared from (S)-1-(4-bromo-3-methyl-phenyl)-ethylamine and triphosgene following a procedure analogous to that described in Step 4 of Intermediate 1. Mass spectrum (ESI+): m/z=272/274 (Br) [M+H+MeOH]+.