反应详情

温度

27.5 °C

Benzylamine (0.927 kg), chloroacetaldehydedimethylacetal (0.909 kg), sodium hydroxide solution (0.35 kg) in 2.72 L of water were charged into the flask under stirring at 25-30° C. for 10-15 min. Reaction mass was heated to 100-102° C. under stirring for 30 hrs. After completion of reaction, reaction mass was allowed to settle for 30 min. Two layers are separated and upper product layer was collected, distilled under high vacuum.

1. customReaction mass
2. temperaturewas heated to 100-102° C.
3. stirringunder stirring for 30 hrs
4. customAfter completion of reaction, reaction mass
5. waitto settle for 30 min
6. customTwo layers are separated
7. customupper product layer was collected
8. distillationdistilled under high vacuum