Sucrose → 61825-94-3

HRID 408064Notes

Reaction equation

HRID 408064 reaction equation
[CH2:1]1[CH2:6][C@@H:5]([NH2:7])[C@H:4]([NH2:8])[CH2:3][CH2:2]1.[C:9]([OH:14])([C:11]([OH:13])=[O:12])=[O:10].[Pt:15].C(O)[C@H]1O[C@H](O[C@]2(CO)O[C@H](CO)[C@@H](O)[C@@H]2O)[C@H](O)[C@@H](O)[C@@H]1O>>[CH2:1]1[CH2:6][C@H:5]2[NH2:7][Pt:15]3([O:13][C:11](=[O:12])[C:9](=[O:14])[O:10]3)[NH2:8][C@@H:4]2[CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 5988SucroseHCID 5310940HCID 5310940, compound

Product 1

HCID 988705461825-94-3

Conditions

Temperature
40 °C

Procedure

An aqueous solution of l-OHP (8 mg/mL, in a 300 mM sucrose solution) was added to about 3.5 g of lyophilized blank liposome and rehydrated by stirring for 2 hours at 40° C. After stirring, liposomal l-OHP was separated from free l-OHP by fractionation using Sephadex G-25 (φ1×45 cm). The liposome l-OHP and free l-OHP were monitored by VIS 600 nm and UV 210 nm respectively.

Workup

  1. stirringAfter stirring
  2. customliposomal l-OHP was separated from free l-OHP by fractionation

Sources & evidence

ORD record
ord-f867c582d2fb46f5a038efb2993dddd8
Source dataset
uspto-grants-2014_06
Patent number
US08758810B2

Reaction notes

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